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Single-Step Plasma-Induced Synthesis of Graphene-Based Nanocomposites

2026-04Artigo científico Acesso aberto
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dc.contributor.authorBundaleska, Neli
dc.contributor.authorFelizardo, Edgar
dc.contributor.authorDias, Ana Amaral
dc.contributor.authorFerraria, Ana Maria
dc.contributor.authordo Rego, Ana M.Botelho
dc.contributor.authorZavašnik, Janez
dc.contributor.authorCvelbar, Uros
dc.contributor.authorBundaleski, Nenad
dc.contributor.authorGuerreiro, Pedro M.A.
dc.contributor.authorTeodoro, Orlando M.N.D.
dc.contributor.authorAbrashev, Miroslav
dc.contributor.authorKissovski, Jivko
dc.contributor.authorAlmeida, Amelia
dc.contributor.authorCarvalho, Patrícia A.
dc.contributor.authorStrunskus, Thomas
dc.contributor.authorGonçalves, Bruno
dc.contributor.authorTatarova, Elena
dc.contributor.institutionDF – Departamento de Física
dc.contributor.institutionCeFITec – Centro de Física e Investigação Tecnológica
dc.contributor.pblMDPI AG
dc.date.accessioned2026-08-18T13:03:01Z
dc.date.available2026-08-18T13:03:01Z
dc.date.issued2026-04
dc.descriptionThe work was supported by the NATO Science for Peace and Security Programme through AEGIS—Advanced Electromagnetic Graphene-based shields via plasma Induced Synthesis Project (Multi-Year Project G7918). M.A. and J.K. acknowledge the financial support by the European Union-Next Generation EU, through the National Recovery and Resilience Plan of the Republic of Bulgaria, project No. BG-RRP-2.004-0008-C01, European Regional Development Fund under “Research Innovation and Digitization for Smart Transformation” program 2021–2027 under the Project BG16RFPR002-1.014-0006 “National Centre of Excellence Mechatronics and Clean Technologies” and INFRAMAT (National Roadmap for Research Infrastructure), supported by Bulgarian Ministry of Education and Science. U.C. and J.Z. acknowledge the Slovenian Research Agency (ARIS) for the projects Z2-4467 and J2-50074, and program No. P1-0417, as well as the EU Graphene Flagship FLAG-ERA III JTC 2021 project VEGA (PR-11938) and M-ERA.NET 3 project ANGSTROM (the project is funded by the Ministrstvo za visoko šolstvo, znanost in inovacije—MVZI, Slovenia). The authors would like to acknowledge the financial support from the European Innovation Council Pathfinder project under grant agreement No. 101046835. Publisher Copyright: © 2026 by the authors.
dc.description.abstractGraphene-based composite materials have attracted much attention for a range of applications in various fields, including electronics, sensing, catalysis, energy storage and conversion. Single-step large-scale microwave plasma synthesis of graphene and nitrogen-doped graphene (N-graphene) composite materials has been demonstrated. The developed atmospheric pressure plasma method allows continuous synthesis of different graphene-based hybrids in a controllable and environmentally friendly manner. Control over the synthesis process, i.e., size, uniformity, surface distribution of the nanoparticles and graphene/N-graphene quality, was provided by adjusting plasma parameters and injection configuration. Protocols for the production of particular composites, i.e., graphene-MnO, N-graphene-MnO, N-graphene-MnS, and N-graphene-FexOy, have been established using methane and acetonitrile as precursors. A comprehensive physicochemical characterization of the produced composites was conducted using high-resolution transmission electron microscopy, scanning transmission electron microscopy, Raman spectroscopy, X-ray diffraction, and near-edge X-ray-absorption fine-structure and X-ray photoelectron spectroscopies.en
dc.description.versionpublishersversion
dc.description.versionpublished
dc.format.extent20
dc.format.extent9637265
dc.identifier.doi10.3390/nano16080473
dc.identifier.issn2079-4991
dc.identifier.otherPURE: 171077221
dc.identifier.otherPURE UUID: 9d57c1b3-ea4e-42ab-896a-ba95389bf358
dc.identifier.otherScopus: 105037077096
dc.identifier.otherORCID: /0000-0002-3424-2847/work/224220607
dc.identifier.otherORCID: /0000-0002-1967-1475/work/224221500
dc.identifier.urihttp://hdl.handle.net/10362/205470
dc.identifier.urlhttps://www.scopus.com/pages/publications/105037077096
dc.language.isoeng
dc.peerreviewedyes
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dc.relationinfo:eu-repo/grantAgreement/FCT/Concurso de avaliação no âmbito do Programa Plurianual de Financiamento de Unidades de I&D (2017%2F2018) - Financiamento Base/UIDB%2F04565%2F2020/PT
dc.relationinfo:eu-repo/grantAgreement/FCT/Concurso de avaliação no âmbito do Programa Plurianual de Financiamento de Unidades de I&D (2017%2F2018) - Financiamento Programático/UIDP%2F04565%2F2020/PT
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dc.relationinfo:eu-repo/grantAgreement/FCT/Concurso de avaliação no âmbito do Programa Plurianual de Financiamento de Unidades de I&D (2017%2F2018) - Financiamento Base/UIDB%2F00100%2F2020/PT
dc.relationinfo:eu-repo/grantAgreement/FCT/Concurso de avaliação no âmbito do Programa Plurianual de Financiamento de Unidades de I&D (2017%2F2018) - Financiamento Programático/UIDP%2F00100%2F2020/PT
dc.relationinfo:eu-repo/grantAgreement/FCT/Concurso para Atribuição do Estatuto e Financiamento de Laboratórios Associados (LA)/LA%2FP%2F0056%2F2020/PT
dc.subjectatmospheric pressure
dc.subjectgraphene composite
dc.subjectmicrowave plasma
dc.subjectN-graphene composite
dc.subjectscalable production
dc.subjectGeneral Chemical Engineering
dc.subjectGeneral Materials Science
dc.titleSingle-Step Plasma-Induced Synthesis of Graphene-Based Nanocompositesen
dc.typejournal article
degois.publication.issue8
degois.publication.titleNanomaterials
degois.publication.volume16
dspace.entity.typePublication
rcaap.rightsopenAccess

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