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Image Recording and Processing Chemical Synthesis

2021-03Artigo científico Acesso aberto
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dc.contributor.authorSousa, David M.
dc.contributor.authorCarlos Lima, João
dc.contributor.authorFerreira, Isabel
dc.contributor.institutionCENIMAT-i3N - Centro de Investigação de Materiais (Lab. Associado I3N)
dc.contributor.institutionDCM - Departamento de Ciência dos Materiais
dc.contributor.institutionDQ - Departamento de Química
dc.contributor.institutionLAQV@REQUIMTE
dc.contributor.pblWiley
dc.date.accessioned2024-07-01T22:32:52Z
dc.date.available2024-07-01T22:32:52Z
dc.date.issued2021-03
dc.descriptionThis work was mainly funded by ERC‐CoG‐2014, ChapTherPV, 647596 and partially by H2020‐ICT‐2014‐1, RIA, TransFlexTeg, 645241, FEDER funds through the COMPETE 2020 Program and National Funds through FCT – Portuguese Foundation for Science and Technology with the reference SFRH/BD/135948/2018. Publisher Copyright: © 2020 The Authors. Published by Wiley-VCH GmbH.
dc.description.abstractThe reproducibility of chemical synthesis is of crucial importance for both chemical industry and research. The development of simple yet robust methods and algorithms that generate a set of data to help the community access their method's reproducibility is desirable. We report a method for obtaining, processing and analyzing recorded images, using scripting language Python 3, from any camera that allows continuous visualization and recording of a chemical synthesis. The method can be used to assert synthesis reproducibility, to capture reaction events that might elude the naked eye and later be isolated in posterior reactions, to refine synthesis parameters such as temperature, microwave power and time and also to understand chemical reactions during synthesis. The method was exemplified with two microwave-assisted synthesis, zinc sulfide and silver sulfide, processed at our lab and applied to videos from other authors.en
dc.description.versionpublishersversion
dc.description.versionpublished
dc.format.extent5
dc.format.extent1424609
dc.identifier.doi10.1002/cmtd.202000043
dc.identifier.otherPURE: 94066643
dc.identifier.otherPURE UUID: a2db6ec6-67f7-4410-a753-a0713fb857ad
dc.identifier.otherScopus: 85166276312
dc.identifier.otherWOS: 001054481400005
dc.identifier.otherORCID: /0000-0002-8838-0364/work/162761792
dc.identifier.otherORCID: /0000-0003-0528-1967/work/162763127
dc.identifier.urihttp://hdl.handle.net/10362/169261
dc.identifier.urlhttps://www.scopus.com/pages/publications/85166276312
dc.language.isoeng
dc.peerreviewedyes
dc.relationFunding Information: info:eu-repo/grantAgreement/EC/H2020/647596/EU
dc.relationinfo:eu-repo/grantAgreement/EC/H2020/645241/EU
dc.relationLarge area transparent thin film thermoelectric devices for smart window and flexible applications
dc.subjectautomation
dc.subjectfeature extraction
dc.subjectimaging
dc.subjectrecording
dc.subjectreproducibility
dc.subjectsynthesis parameters
dc.subjectElectrochemistry
dc.subjectSpectroscopy
dc.subjectCatalysis
dc.subjectFluid Flow and Transfer Processes
dc.titleImage Recording and Processing Chemical Synthesisen
dc.title.subtitleMethod Description and Demonstrationen
dc.typejournal article
degois.publication.firstPage157
degois.publication.issue3
degois.publication.lastPage161
degois.publication.titleChemistry-Methods
degois.publication.volume1
dspace.entity.typePublication
oaire.awardNumber645241
oaire.awardNumberSFRH/BD/135948/2018
oaire.awardTitleLarge area transparent thin film thermoelectric devices for smart window and flexible applications
oaire.awardURIinfo:eu-repo/grantAgreement/EC/H2020/645241/EU
oaire.awardURIinfo:eu-repo/grantAgreement/FCT/OE/SFRH%2FBD%2F135948%2F2018/PT
oaire.fundingStreamH2020
oaire.fundingStreamOE
project.funder.identifierhttp://doi.org/10.13039/501100008530
project.funder.identifierhttp://doi.org/10.13039/501100001871
project.funder.nameEuropean Commission
project.funder.nameFundação para a Ciência e a Tecnologia
rcaap.rightsopenAccess
relation.isProjectOfPublicationda4dcbfc-0fcc-41cc-b5dc-98cb44daf18a
relation.isProjectOfPublicationa80aa8d8-b158-4c75-9efb-35ef9edf8047
relation.isProjectOfPublication.latestForDiscoverya80aa8d8-b158-4c75-9efb-35ef9edf8047

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